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纳米管的电子显微分析
作者：王中林等编
出版社：清华大学出版社
出版时间：2004-03-01
ISBN：9787302082132
定价：¥78.00
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内容简介
碳纳米管的研究已经进行了13年之久。碳纳米管已成为纳米科学和技术研究和发展中一种独特而且具有代表性的材料。目前有关碳纳米管的合成和性能表征方面的书籍已有几本。作为发现碳纳米管的第一手段，高分辨透射电子显微镜在整个碳纳米管的研究中起了关键的作用，但介绍如何利用电子显微镜分析碳纳米管方面的书籍却没有。考虑到大量读者的需求，我们在2003年编辑的英文版《Electron Microscopy of Nanotubes》一书主要是介绍透射电子显微镜在分析和测试管形纳米结构中的方法和应用。本书集结了世界范围内在应用透射电子显微镜进行纳米管研究方面的专家编写出这一独特的科技参考书。希望本书能对从事纳米管研究方面的科技工作者和学生有所帮助。
作者简介
暂缺《纳米管的电子显微分析》作者简介
目录
Part I. Diffraction, Imaging, and Spectroscopy of
Carbon-Based Nanotubes
1. Diffraction and Imaging of Single-Walled Carbon Nanotubes
L.-C. Qin
1.1 Introduction
1.2 Structure Description
1.3 Morphological Study
1.4 Determination of Helicity
1.5 Discussion
1.6 Summary
i.7 Appendix
2. Electron Diffraction and Microscopy of Single-Walled
Carbon Nanotube Bundles
J.-F. Colomer and G. Van Tendeloo
2.1 Introduction
2.2 Direct Observation of SWNT Bundles
2.3 Electron Diffraction of SWNT Bundles
2.4 SWNT Bundles Produced by Different Methods
2.5 Discussion
2.6 Conclusions
3. Nanodiffraction of Carbon Nanotubes
J. M. Cowley
3.1 Introduction
3.2 Nanodiffraction from Single-Walled Nanotubes
3.3 Ropes of Nanotubes
3.4 Multiwalled Nanotubes (MWnT)
3.5 Nanoshells
3.6 The Use of Nanotubes and Nanoshells for Imaging Experiments
3.7 Conclusions and Discussion
4. The Smallest Carbon Nanotubes
N. Wang
4.1 Introduction
4.2 How Small can Carbon Nanotubes be?
4.3 Ultrasmall Carbon Nanotubes
4.4 TEM Contrast of the Innermost Tube in 0.4 nm
Multiwalled Carbon Nanotubes
4.5 Novel Properties of 0.4 nm Single-Walled Carbon Nanotubes
4.6 Summary
5. Electron Energy-Loss Spectroscopy of
Carbon Nanotubes and Onions
T. Stockli
5.1 Introduction
5.2 Plasmon Losses
5.3 Core Losses
5.4 Concluding Remarks
6. Carbon Nanostructures Under the Electron Beam:
Formation of New Structures and In-Situ Study of
Radiation-Induced Processes
S. Trasobares and P. M. Ajayan
6.1 Introduction
6.2 Electron Beam Effect on Graphite, Carbon Nanotubes, and Onions
6.3 Using the Microscope as a Nano-Laboratory for Creating
New Structures
6.4 In-Situ Activation and Property Measurements of Carbon Nanotubes
with the Electron Beam
6.5 Conclusions
Part II. Nanomeasurements of Carbon Nanotubes
based on In-Situ TEM
7. ln-Situ Mechanical Properties of Nanotubes and Nanowires
Z. L. Wang
7.1 Static Mechanical Properties of Carbon Nanotubes by
Atomic Force Microscopy
7.2 Measuring Dynamic Bending Modulus by Electric
Field-Induced Mechanical Resonance
7.3 Young's Properties of Composite Nanowires
7.4 Summary
8. In-Situ Field Emission of Carbon Nanotubes
Z. L. Wang
8.1 The Fowler-Nordheim Equation for Field Emission
8.2 Field Emission from Arrays of Carbon Nanotubes
8.3 Work Function at the Tips of Carbon Nanotubes
8.4 Electrostatic Charges on Carbon Nanotubes
8.5 Mapping the Electrostatic Potential at the Nanotube Tips
8.6 Field Emission-Induced Structural Damage
8.7 Nanothermometer and Nanobearing
8.8 Summary
9. In-Situ Electric Transport of Carbon Nanotubes
Z. L. Wang, P. Poncharal, W. A. de Heer, and C. Hui
9.1 Ballistic Quantum Conductance: What is it?
9.2 Ballistic Quantum Conductance at Room Temperature
9.3 ln-Situ Measurements
9.4 Quantum Conductance and Surface Contamination
9.5 Top-Layer Transport in MWNT
9.6 Summary
Part III. Tubular Structures and Nanocrystals Grown by
Filling Nanotubes
10. Electron Microscopy of Boron Nitride Nanotubes
D. Golberg and Y. Bando
10.1 Introduction
10.2 Morphology of BN NTs as Revealed by HRTEM
10.3 BN NT Helicity and Atomic Structure as Revealed by HRTEM
and Electron Diffraction
10.4 Electron Microscopy of Filled BN NTs
10.5 In-Sim TEM Observations of BN NT Electron-Irradiation-
Induced Changes
10.6 Electron-Energy Loss Spectroscopy and Energy-Filtered Elecm
Microscopy of BN and C-Doped BN NTs
10.7 Summary
11. Inorganic Nanoparticles with Fu!!erene-like Structure and
Inorganic Nanotubes
R. Tenne and R. Popovitz-Biro
11.1 Introduction
11.2 Classification of the Folding Mechanisms of Inorganic Compou
which Lead to Close Cage Structures and Nanotubes
11.3 Thermodynamic, Structural, and Topological Considerations
11.4 Transmission Electron Microscopy Studies of Nanotubes
11.5 Conclusions
12. Integral Atomic Layer Architectures of ID Crystals Inserted into
Single-Walled Carbon Nanotubes
d. Sloan, A. 1. Kirkland, J. L. Hutchison, and M. L. H. Green
12.1 Introduction
12.2 Synthesis of l D Crystals within SWNTs
12.3 Computer Simulations of 2 ~ 2 and 3 ~ 3 KI Crystals in
Variable Diameter SWNT
12.4 ID Crystals Derived from Polyhedral Framework Structures
12.5 1D BaI2 Chain with Five- and Six-Coordination
12.6 Halide Cluster Formation Within SWNTs
12.7 Imaging and Electron Energy Loss Spectroscopy of a ID
"Metastable Ternary Halide Structure
12.8 Molecules Meet Crystals: Simultaneous Observation of 1D
Crystals and Fullerenes within SWNTs
12.9 Conclusions
Carbon-Based Nanotubes
1. Diffraction and Imaging of Single-Walled Carbon Nanotubes
L.-C. Qin
1.1 Introduction
1.2 Structure Description
1.3 Morphological Study
1.4 Determination of Helicity
1.5 Discussion
1.6 Summary
i.7 Appendix
2. Electron Diffraction and Microscopy of Single-Walled
Carbon Nanotube Bundles
J.-F. Colomer and G. Van Tendeloo
2.1 Introduction
2.2 Direct Observation of SWNT Bundles
2.3 Electron Diffraction of SWNT Bundles
2.4 SWNT Bundles Produced by Different Methods
2.5 Discussion
2.6 Conclusions
3. Nanodiffraction of Carbon Nanotubes
J. M. Cowley
3.1 Introduction
3.2 Nanodiffraction from Single-Walled Nanotubes
3.3 Ropes of Nanotubes
3.4 Multiwalled Nanotubes (MWnT)
3.5 Nanoshells
3.6 The Use of Nanotubes and Nanoshells for Imaging Experiments
3.7 Conclusions and Discussion
4. The Smallest Carbon Nanotubes
N. Wang
4.1 Introduction
4.2 How Small can Carbon Nanotubes be?
4.3 Ultrasmall Carbon Nanotubes
4.4 TEM Contrast of the Innermost Tube in 0.4 nm
Multiwalled Carbon Nanotubes
4.5 Novel Properties of 0.4 nm Single-Walled Carbon Nanotubes
4.6 Summary
5. Electron Energy-Loss Spectroscopy of
Carbon Nanotubes and Onions
T. Stockli
5.1 Introduction
5.2 Plasmon Losses
5.3 Core Losses
5.4 Concluding Remarks
6. Carbon Nanostructures Under the Electron Beam:
Formation of New Structures and In-Situ Study of
Radiation-Induced Processes
S. Trasobares and P. M. Ajayan
6.1 Introduction
6.2 Electron Beam Effect on Graphite, Carbon Nanotubes, and Onions
6.3 Using the Microscope as a Nano-Laboratory for Creating
New Structures
6.4 In-Situ Activation and Property Measurements of Carbon Nanotubes
with the Electron Beam
6.5 Conclusions
Part II. Nanomeasurements of Carbon Nanotubes
based on In-Situ TEM
7. ln-Situ Mechanical Properties of Nanotubes and Nanowires
Z. L. Wang
7.1 Static Mechanical Properties of Carbon Nanotubes by
Atomic Force Microscopy
7.2 Measuring Dynamic Bending Modulus by Electric
Field-Induced Mechanical Resonance
7.3 Young's Properties of Composite Nanowires
7.4 Summary
8. In-Situ Field Emission of Carbon Nanotubes
Z. L. Wang
8.1 The Fowler-Nordheim Equation for Field Emission
8.2 Field Emission from Arrays of Carbon Nanotubes
8.3 Work Function at the Tips of Carbon Nanotubes
8.4 Electrostatic Charges on Carbon Nanotubes
8.5 Mapping the Electrostatic Potential at the Nanotube Tips
8.6 Field Emission-Induced Structural Damage
8.7 Nanothermometer and Nanobearing
8.8 Summary
9. In-Situ Electric Transport of Carbon Nanotubes
Z. L. Wang, P. Poncharal, W. A. de Heer, and C. Hui
9.1 Ballistic Quantum Conductance: What is it?
9.2 Ballistic Quantum Conductance at Room Temperature
9.3 ln-Situ Measurements
9.4 Quantum Conductance and Surface Contamination
9.5 Top-Layer Transport in MWNT
9.6 Summary
Part III. Tubular Structures and Nanocrystals Grown by
Filling Nanotubes
10. Electron Microscopy of Boron Nitride Nanotubes
D. Golberg and Y. Bando
10.1 Introduction
10.2 Morphology of BN NTs as Revealed by HRTEM
10.3 BN NT Helicity and Atomic Structure as Revealed by HRTEM
and Electron Diffraction
10.4 Electron Microscopy of Filled BN NTs
10.5 In-Sim TEM Observations of BN NT Electron-Irradiation-
Induced Changes
10.6 Electron-Energy Loss Spectroscopy and Energy-Filtered Elecm
Microscopy of BN and C-Doped BN NTs
10.7 Summary
11. Inorganic Nanoparticles with Fu!!erene-like Structure and
Inorganic Nanotubes
R. Tenne and R. Popovitz-Biro
11.1 Introduction
11.2 Classification of the Folding Mechanisms of Inorganic Compou
which Lead to Close Cage Structures and Nanotubes
11.3 Thermodynamic, Structural, and Topological Considerations
11.4 Transmission Electron Microscopy Studies of Nanotubes
11.5 Conclusions
12. Integral Atomic Layer Architectures of ID Crystals Inserted into
Single-Walled Carbon Nanotubes
d. Sloan, A. 1. Kirkland, J. L. Hutchison, and M. L. H. Green
12.1 Introduction
12.2 Synthesis of l D Crystals within SWNTs
12.3 Computer Simulations of 2 ~ 2 and 3 ~ 3 KI Crystals in
Variable Diameter SWNT
12.4 ID Crystals Derived from Polyhedral Framework Structures
12.5 1D BaI2 Chain with Five- and Six-Coordination
12.6 Halide Cluster Formation Within SWNTs
12.7 Imaging and Electron Energy Loss Spectroscopy of a ID
"Metastable Ternary Halide Structure
12.8 Molecules Meet Crystals: Simultaneous Observation of 1D
Crystals and Fullerenes within SWNTs
12.9 Conclusions
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